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Graywolf

Qwet Oil Extraction

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Quick Wash Ethanol, also know as QWET is one of the techniques commonly employed to extract oil from cannabis.

 

Here is skunk pharm’s QWET formula to produce an absolute using a 3 minute quick wash.

 

As most of our extracted oil goes into oral meds, we also decarboxylate ours. This process is based on the 252F curve shown in the attached graph.

 

The first question is why use a quick wash technique to extract the resins, instead of long soaks to extract as much resin as possible, or just boiling the material in alcohol to get the greatest amount of extracted material?

 

The answer to that is that because alcohol is a highly polar solvent that is soluble in water, the latter two techniques also extract the water solubles like chlorophyll and plant alkaloids, as well as the plant waxes and vegetable oil.

 

Even quick wash does to a lesser degree, but the added steps that we include here minimize pickup even further and we take additional steps to remove the impurities that we do pick up.

 

The first wash will usually extract 75 to 80%, leaving the balance for the second. The second extraction will be more sedative and less heady. If you use a hand microscope, you can easily see when the trichome heads are gone and the stalks look like wet fur.

 

You can also use the material for other extraction methods after it has dried. I have subsequently used BHO after the first QWET wash that yielded 16% oil by weight, and got 5% more pristine oil, or about 21.6% total.

 

A cured material QWET absolute is one of the most aromatic and tasty of the extraction methods and consistently gets high raves from the volunteer test panels, as well as the patients and students. Both from an efficacy, as well as a flavor standpoint.

 

The first step in the process is to get as much water as possible out of the material.

 

A fresh material QWET is possible, but this procedure is specifically for material that has been cured to about 15% water content, which is typical of cured material. 15% is a lot of water and the alcohol already has 5% in it, so unless we reduce the water content even further, we will be extracting a lot of water solubles.

 

We dry our cured material even further by spreading it on a cookie sheet and baking it in a 200F oven until just frangible when rolled between the finger and thumb.

 

If the material is prime bud, we break it up loosely by hand and extract from trim as is.

 

We never, ever, use a blender or coffee grinder to reduce material, because it produces a lot of ultra fine powder that makes it through conventional filters.

 

Next, while it is still warm, we seal the material in a jar, which we place in the freezer to tie up any remaining water as ice. We also put the 190 proof grain alcohol in the freezer.

 

When they have both stabilized at about 0F, pour the alcohol into the jar of plant material, so that it is at least an inch above the material, and shake it gently a few times to make sure everything is wet. Place back in the freezer.

 

Remove and gently shake twice more until the material has soaked for 3 minutes, and then dump it through a wire strainer to drain quickly.

 

Set the material aside to dry for a second extraction. We usually keep the two extractions separate, as they will have different properties.

 

Filter the extracted liquid.

 

We use either a #1 lab filter with a vacuum assist, or a simple coffee filter, depending on the quantity we are processing.

 

Place that filtered liquid in a suitable container and set that container in an oil bath heated to 250F. We use bain marie and other stainless ware from a restaurant supply or a still, so as to recover the alcohol.

 

Make sure that the container is sitting on something that suspends it up off the bottom of the oil pot. I throw four jar lids in the bottom of my electric fondue pot and use it for that purpose.

 

Never trust the numbers on the dial and use a good thermometer to set temperatures. We use either a mercury lab thermometer, or a digital one. Good temperature control is key to the process.

 

That means the device that you use to control the oil temperature must have a narrow dead band, so that the temperature control is stable.

 

I paid about $60 for a Quisinart fondue pot that was designed to heat sensitive sauces like chocolate and has excellent control throughout its temperature range. There are a couple of Revels in our group that are slightly larger and work well, plus cost only about $30, though they have a slightly larger dead band.

 

Some fry cookers have sensitive enough controls, but many deep fryers designed to primarily run at 375F, lack control sensitivity and have large dead bands at 250F.

 

Either boil or distill off the alcohol until the liquid is reduced to a pool of oil, with no large solvent bubbles.

 

The oil is useable at this point, but to make an absolute out of it, we wash it out of the pot with at least ten volumes of alcohol and using a funnel, pour that liquid into a jar or bottle, seal it, and place that in the freezer.

 

If you leave it overnight at -30F, the liquid will lose its clarity and become slightly cloudy, primarily from plant waxes flocculating out.

 

Filter that liquid one more time, and you will have a bell clear extract, that is ready to reduce down one more time.

 

We suck it out of the container using a 60ml syringe, and then filter it to 0.2 microns using a syringe filter, but a coffee filter or a #1 lab filter may be used..

 

Place in a suitable container for return to the oil bath and this time cook it until there are not only no large alcohol bubbles, but the production of small CO2 bubbles along the edge dramatically slows down, even when stirred with a bamboo skewer.

 

Since you have much less material, a smaller one may be used. At this point I put them in small stainless cups with their tare engraved on their sides or a Pyrex beaker. The smaller container reduces the surface area that will be coated with oil when I cook it down the last time and knowing the cups tare weight allows me to take it directly from the oil bath and place it on a scale after simply wiping the exterior.

 

Since I know the tare, I then know the extracted weight, and exactly how much other ingredients to add. Once adding those ingredients, I place the cup back in the oil bath, where I stir it until well mixed and then decant into its final container.

 

Since the added ingredients include things that lower the cannabis oils viscosity, very little is left as a film in that container.

 

If I plan to use the oil as is, without adding any other ingredients, I extract it from the container using the syringe, or a pipette, so as to not leave a streak of material in the vessel. After I have extracted all that I can using a syringe or pipette, I wash the container and pipette out with hot alcohol, and save the wash for the next run.

 

Nothing is wasted or left behind.

 

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it is really quite easy and requires very little in equipment. can be don in fairly tight quarters. inexpensive too, if using iso.

 

 

True, true! Easy and little equipment required, if you are not trying to recover the alcohol. Even if you are, pot stills are easy to make!

 

I will also post a QWISO process, which as ES notes is cheaper than using ethanol.

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True, true! Easy and little equipment required, if you are not trying to recover the alcohol. Even if you are, pot stills are easy to make!

 

I will also post a QWISO process, which as ES notes is cheaper than using ethanol.

Is there a link for "How to make a pot still" anywhere? :jumping0041: Thanks


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Keep in mind that anytime you operate a still and RECOVER the alcohol, it is very illegal. Let the alcohol evaporate instead and you're legal.

 

The government doesn't like people not paying the ridiculously high taxes they impose on booze, and you'll rot in prison if they catch you. And they don't care what type of alcohol it is. Alcohol is alcohol when a still is involved.


 

                                                                                                                                                   

 

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Point well made. There are laws against producing distilled spirits without a license. Proceed here on your own and see your personal attorney for professional advice.

 

I interpret the law as saying that I can't produce distilled spirits or alcohol fuel without a distillers license. I don't see where it proscribes me recovering alcohol that I have already paid the taxes on.

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JD,

I agree with you. Already paid taxes on it, it should be ours to do with as we please.

 

 

Unfortunately a federal judge isn't likely to interpret the law in the same way you or I do. In fact, the ATF's website clearly says that recovering alcohol from a still (even if you already paid taxes on it) is illegal. I personally prefer to err on the side of caution whenever possible. Aside from my own selfish desire to remain "free", I have children that really need their daddy to not be in prison. LOL


 

                                                                                                                                                   

 

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The ATF site also has the following:

 

"Small stills (with a cubic distilling capacity of a gallon or less) that are used for laboratory purposes or for distilling water or other non-alcoholic materials are exempt from our rules."

 

I believe the intent of the law is to prevent people from making untaxed alcoholic beverages and the ATF storm troopers are unlikely to kick down our laboratory doors for a still under a gallon capacity recycling alcohol for medical extractions.

 

Having said that, I am not a lawyer and could be wrong. I encourage everyone to get their legal advice from someone qualified.

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also, as i read the law, there is a section allowing for reclaim if taxes were originally paid. i doubt they are coming after an alcoholic reclaiming solvent from concentrates.

 

honestly, most of the time, we are using ethanol in clean up. reclaim is hardly worth it there. since skunk pharmers figured out how to make sedative meds from butane honey oil (minimizing chlorophyll), i have not done a reflux, so have not needed to use my recovery system.

 

obviously, i haven't done any qwet either.

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The ATF site also has the following:

 

"Small stills (with a cubic distilling capacity of a gallon or less) that are used for laboratory purposes or for distilling water or other non-alcoholic materials are exempt from our rules."

 

I believe the intent of the law is to prevent people from making untaxed alcoholic beverages and the ATF storm troopers are unlikely to kick down our laboratory doors for a still under a gallon capacity recycling alcohol for medical extractions.

 

Having said that, I am not a lawyer and could be wrong. I encourage everyone to get their legal advice from someone qualified.

Great impute here thanks GW

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